Experiment #3

[kelszo...@msn.com]

I performed a simple dilution with methyl acetate and ethyl acetate.

Sample # Refractive Index Temperature (°C)
1 N/A 60
2 1.365 63
3 1.366 64
4 1.367 66
5 1.368 68
6 1.370 64
7 1.372 63

-Kelsey Smith

[Jessica Tingle]

Mine was a simple distillation with methyl acetate and n-butyl
acetate.

Sample # B.P. Range Refractive Index

1 60-67 1.362
2 67-71 1.363
3 71-76 1.365

4 76-91 1.365
5 91-121 1.390

6 121-122 1.393
7 122-123 1.393
8 123-124 1.393

-Jessica Tingle

[Keli Thurston]

Hello all,

I performed a fractional distillation with the corundum chips using
the mixture with n-butyl acetate

Test tube, temperature when removed, RI

1 54 1.3605
2 54 1.3605
3 54 1.361
4 118 1.3925
5 119 1.3925
6 119 1.393
7 119 1.393

- Keli

[jy3...@gmail.com]

Hello everyone,

Here is my data from a simple distillation of methyl acetate and n-
butyl acetate. Enjoy!

Test Tube # Temperature Range (°C) Refractive Index
1 (3mL) 54-61 1.3645
2 (6mL) 61-66 1.3645
3 (9mL) 66-69 1.3665
4 (12mL) 65-118 1.3930
5 (15mL) 118-120 1.3935
6 (18mL) 120-120 1.3935
7 (21mL) 120-120 1.3940
8 (<24mL) 120-120 1.3950

-Jeffrey Yeung

[Aisha Sindhu]

Hey everyone!

I had a fractional distillation using glass beads, with methyl acetate
and ethyl acetate.

Test Tube # Volume (mL) Temp Range
(Celsius) Refractive Index
1 3
54-59 1.363
2 6
59-59 1.3645
3 9
59-61 1.3645
4 12
61.5-63 1.365
5 15
63.5-67 1.366
6 18
67-71.5 1.370
7 21
71.5-73 1.371


-Aisha Sindhu :)

[K.D. Wu]

Fractional distillation with vigreux with methyl acetate:ethyl acetate

Test tube # BP range (C) Refractive index
1 60-61 1.3650
2 61-61 1.3666
3 61-63 1.3664
4 67-68 1.3690
5 69-72 1.3716
6 72-73 1.3726

[Monica Tain]

Hi, I performed the first variation (methyl acetate with ethyl
acetate)

Volume of Distillate (mL) Temperature (°C) Refractive Index
0-3 55.5-60.0 1.3639
3-6 60.0-61.0 1.3640
6-9 61.0-62.5 1.3645
9-12 62.5-63.5 1.3650
12-15 63.5-64.5 1.3664
15-18 64.5-66.5 1.3675
18-21 66.5-70.0 1.3695
21-22.4 70.0-70.0 1.3705

[Sally Wong]

I performed a fractional distillation with the Vigreux column with
methyl acetate: n-butyl.

Start Temp: 45

Volume of Distillate (mL) Temperature Refractive
Index
3 mL 53.5
1.360
6 mL 55.0
1.361
9 mL 112.0
1.376
12 mL 115.0
1.394
15 mL 116.0
1.395
18 mL 116.0
1.394
21 mL 115.5
1.394

[Sally Wong]

Oh my formatting kind of got messed up, but the number under each
volume value is the refractive index of that sample. The temperatures
are lined up fine.

[Diana Wee]

I performed a simple dilution with methyl acetate and n-propyl. Sample #        Refractive Index        Temperature range (°C) 1                       1.365                      49-62 2                       1.367                      62-65 3                       1.369                      65-65 4                       1.373                      65-66 5                       1.381                      67-73 6                       1.384                      74-78 7                       1.3842                    78-79 8                       1.3842                    79-65 -Diana Wee

[Mark Tai]

Hi all,
I performed a fractional distillation with glass beads on n-propyl
acetate.

Sample # BP Range Refractive Index
1 57-54 1.363
2 54-51 1.364
3 50-55 1.362
4 55-58 1.363
5 58-89 1.369
6 89-117 1.382

Temperature dropped while collecting the first two samples because
heat was turned down
significantly after the 3mL portions started collecting too fast. The
sample boiled over at
the end and dropped to 51C after sample 6, which was only about 2mL.

[Daniel Wexler]

I performed a fractional distillation with chore boy 1:1 methyl
acetate/ ethyl acetate


Fraction # Temp °C Refractive index
1 45 1.366
2 30 1.3655
3 63 1.366
4 65 1.367
5 66 1.3685
6 64 1.371
7 64 1.3735

[Kevin Sun]

Vigreux distillation with methyl acetate and n-propyl


Sample Temperature range Refractive Index
1 (3 ml) 51 56 1.3640
2 (3 ml) 56 59 1.3645
3 (3 ml) 59 62 1.3650
4 (3 ml) 62 77 1.3680
5 (3 ml) 77 95 1.3825
6 (3 ml) 95 96 1.3850
7 (3 ml) 96 97 1.3850

- Kevin Sun

[Marjan Zaman]

I did a simple distillation of methyl acetate and n-propyl acetate. my
temperatures were measured after each tube was collected

Sample Temperature Refractive Index
1 (3 ml) 57 1.3660
2 (3 ml) 66 1.3660
3 (3 ml) 69 1.3670
4 (3 ml) 60 1.3775
5 (3 ml) 85 1.3790
6 (3 ml) 95 1.3840
7 (3 ml) 96 1.3850

[Chris Song]

I did a fractional distillation with carborundum chips of methyl
acetate and n-propyl acetate

Sample             Temperature range                   Refractive
Index
1 (3 ml)                     52-54                            
1.362
2 (3 ml)                     54-54                            
1.3624
3 (3 ml)                     54-56                            
1.363
4 (3 ml)                     56-97                            
1.384
5 (3 ml)                     97-98                            
1.384
6 (3 ml)                     98-100                            
1.3851
7 (3 ml)                     100-100                          
1.3851

[Jacqueline Watkins]

I did a fractional distillation using choreboy. Methyl Acetate with n-
propyl acetate.

Sample Temp. Range Refractive Index
1 55-59 1.3636
2 59-61 1.3639
3 61-61 1.3639
4 61-98 1.3842
5 98-98 1.3853
6 98-98 1.3853
7 98-99 1.3851