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<Sediment.jpg><CaCh_Test.jpg>
Paul,
I had a similar problem this year. Apples which in previous years successfully
keeved failed this year. Their pH was 3.2,
lower than previous years probably due to poor growing conditions. I also did cold maceration for 24 hrs and got
a very strong positive pectin test. I added
PME and circulated the treated juice for 24 hrs at 10 deg C to ensure adequate
contact and reaction time. When I added CaCl,
the rapid formation of gel globules did not take place.
I put a one liter sample in a milk bottle so I could monitor the progress. A murky brown sediment which looked exactly like yours sank to the bottom within 24 hrs. As fermentation got under way, the bubbles streamed out of the sediment leaving tracks like worm holes against the glass of my sample bottle. I concluded that the sediment lacked the gel strength to trap the bubbles and form a chapeau.
I increased the CaCl in the sample to no avail. I added more PME even though I did not expect that to help. It didn't so I racked off the relatively clear juice before it was too late. As this batch ferments, it has coughed up cotton balls of weak gel which I carefully pump out. I should have done a bench test to confirm that keeving would succeed.
In a case like this, I wonder if it would help to increase the pH with calcium bicarbonate prior to PME treatment. Or, would it inhibit the activity of PME?
Tom