stupid clarifier tricks
Dave Whitman
the crystal clear beers I'm getting. I was previously using gelatine
added at bottling time, but feel the irish moss works better.
I had a slip of memory on my last batch, and used IM in the boil but then
also added gelatine during bottling. Don't ask me why; the beer was
already very clear from the irish moss treatment.
This turned into a real disaster. About 3 days after bottling, every
bottle of my previously clear beer has about 0.5 cm of trub
almost-but-not-quite settling to the bottom. Apparently excess irish moss
was still in solution, and is happily doing it's job of precipitating high
molecular weight proteins (the gelatine) into disgusting fluffy trub.
The take home lesson here is to use either irish moss or gelatine, but not
both. Particularly don't add gelatine to an irish moss treated batch at
bottling time.
--
dave whitman Drinking through clenched teeth.
dwhi...@rohmhaas.com "The opinions expressed are those of the
author, and not Rohm and Haas Company."
Geoff Scott
dwhi...@rohmhaas.com (Dave Whitman) wrote:
>
> I had a slip of memory on my last batch, and used IM in the boil but then
> also added gelatine during bottling. Don't ask me why; the beer was
> already very clear from the irish moss treatment.
>
> This turned into a real disaster. About 3 days after bottling, every
> bottle of my previously clear beer has about 0.5 cm of trub
> almost-but-not-quite settling to the bottom.
Sorry to hear about Dave's bad experience but I've done over one hundred
batches that used both gelatine and irish moss. Not been a problem.
regards,
Geoff Scott
gsc...@io.org
Brewing page http://www.io.org/~gscott
Rick Hawkins
Dave Whitman <dwhi...@rohmhaas.com> wrote:
>I had a slip of memory on my last batch, and used IM in the boil but then
>also added gelatine during bottling. Don't ask me why; the beer was
>already very clear from the irish moss treatment.
I once saw a friends batch in which he'd forgotten the irish moss. He
added to his glass fermenter, still cloudy, a few days later. After a
couple of days, there was s distinct line between clear beer above and
still cloudy beer below.
--
R E HAWKINS
rhaw...@iastate.edu
Steve Delorme
In a previous posting, Dave Whitman (dwhi...@rohmhaas.com) writes:
> I recently started adding irish moss to my boils, and am very pleased with
> the crystal clear beers I'm getting. I was previously using gelatine
> added at bottling time, but feel the irish moss works better.
>
> also added gelatine during bottling. Don't ask me why; the beer was
> already very clear from the irish moss treatment.
>
Well I was making a brew a week ago and realized I had no irish moss so I
looked in the fridge for something I could substitute. And well what the
heck I used some celery leaves! I don't know what affect this will have I
my brew, but I'll chalk this one up to a momentary lapse of reason. The
beer started fermenting within an hour, and seems to be ok. Does anyone
have any ideas on what will become of this beer in the long-term?
--
"blurp, blurp"
Dave Whitman
(Geoff Scott) wrote:
> In article <dwhitman-120...@krell.sh.rohmhaas.com>,
> dwhi...@rohmhaas.com (Dave Whitman) wrote:
> >
> > I had a slip of memory on my last batch, and used IM in the boil but then
> > also added gelatine during bottling. Don't ask me why; the beer was
> > already very clear from the irish moss treatment.
> >
> > This turned into a real disaster. About 3 days after bottling, every
> > bottle of my previously clear beer has about 0.5 cm of trub
> > almost-but-not-quite settling to the bottom.
>
> Sorry to hear about Dave's bad experience but I've done over one hundred
> batches that used both gelatine and irish moss. Not been a problem.
Actually I've used both in a batch before with sucess myself. I think
what went wrong with THIS batch was adding the gelatine at bottling,
WITHOUT adding some into the secondary and allowing settling of the irish
moss / gelatine adduct. Do you add your gelatine to secondary, or only at
bottling time?
I'll be doing an experiment this weekend to confirm, but based on their
chemistries, I expect that solutions of IM and gelatine which would be
stable in isolation will produce a precipitate when combined. If this
reaction is allowed to happen in the secondary, everything settles out,
and a subsequent addition of gelatine at bottling time is no problem since
excess IM has already been removed.
Does this make sense, or am I out in left field somewhere? Can you think
of another explanation for the room temperature trub formation in my
bottles after a 2 week secondary, with clean looking beer going into the
bottles?
--
dave whitman "The opinions expressed are those of the
dwhi...@rohmhaas.com author, and not Rohm and Haas Company."
They made me say that. Really.
The Newt King
>
>>I had a slip of memory on my last batch, and used IM in the boil but then
>>also added gelatine during bottling. Don't ask me why; the beer was
>>already very clear from the irish moss treatment.
>
>added to his glass fermenter, still cloudy, a few days later. After a
>couple of days, there was s distinct line between clear beer above and
>still cloudy beer below.
>--
>R E HAWKINS
>rhaw...@iastate.edu
I thought that Irish Moss and gelatine did two different things. The Irish
Moss
settled out the proteins which cause chill haze and the gelatine helps settle
out the yeast and cause the yeast cake in the bottom of the bottle to be more
stable. I've always used both and great results (including clear wheat beers).
The Newt King
The Newt King
>In article <gscott-1505...@gscott.net2.io.org>, gsc...@io.org
>> >
>> > I had a slip of memory on my last batch, and used IM in the boil but then
>> > also added gelatine during bottling.
>>
>> batches that used both gelatine and irish moss. Not been a problem.
>
>Actually I've used both in a batch before with sucess myself. I think
>what went wrong with THIS batch was adding the gelatine at bottling,
>WITHOUT adding some into the secondary and allowing settling of the irish
>moss / gelatine adduct. Do you add your gelatine to secondary, or only at
>bottling time?
>
I also do a secondary where probally most of the IM is removed along with the
trub.
I've done probally close to 60 batchs with no problem.
The Newt King
Christopher Tkach
questions for me.
How does it work?
How much is needed for five gallons?
Is regular grocery store bought Gelatin good enough to use?
Which is better to use Irish Moss or Gelatin?
Thanks,
- Chris
Dave Whitman
Tkach) wrote:
I've been thinking a lot about this lately and looking into the chemistry of clarifiers, so forgive a long (but hopefully information-rich) post.
There are two main mechanisms by which beer can be cloudy: suspended yeast and protein/polyphenol chill haze complex. (Actually 3, but I won't talk about starch haze which applies only to all-grain brewing).
Gelatine is a high molecular weight protein that helps agglomerate and precipitate suspended yeast. It does not eliminate chill haze, and may even make it worse (see below for speculation about this). Although gelatine helps yeast precipitate, sufficient yeast remains in the beer to allow carbonation and bottle conditioning.
Irish moss removes high molecular weight proteins. High molecular weight proteins can combine with polyphenols which are also present in beer to form a complex. This complex is soluble at room temperature, but precipitates out upon cooling, forming chill haze. Removing the proteins stops the complex formation and thus reduces haze. Irish moss has no effect on suspended yeast.
Polyclar 10 is a selective adsorbant for polyphenols, the other half of the chill haze complex. Adding Polyclar 10 is thus another way to reduce chill haze. It is also supposed to help agglomerate yeast, although in my experience, gelatine works better for that. Since polyphenols contribute to beer color, your beer may have a slightly lighter color after adding polyclar.
*******
Usage notes:
Gelatine: The stuff in the grocery store is identical to that in brewing shops, but cheaper. Add 1 tsp or 1 packet of gelatine to a cup of boiling water, boil 5 minutes to sanitize, cool to room temperature. If you use a secondary, add the solution after racking. Otherwise, add the solution in your bottling bucket just before bottling.
Irish Moss: Add 1 TBSP of irish moss to a cup of water a few hours before you brew, to hydrate it (it'll swell up dramatically, but won't dissolve). Add the hydrated material to your boil during the last 15 minutes. In your fermenter, you'll see weird-blobs-of-goo floating around after everything cools off. This is normal, showing that the moss is doing its job of precipitating out proteins.
Polyclar 10: It's an insoluble white powder. Boil a cup of water, add 1 TBSP polyclar and boil 5 minutes to sanitize (it won't swell or dissolve). Cool to room temperature, swirl to suspend the powder and add to secondary AFTER racking your beer (you want the polyclar to pass through the beer as it settles). Don't add at bottling time or you'll have a lot of powdery gunk at the bottom of your bottles.
*******
Speculations about combining clarifiers:
Chemically, it doesn't make much sense to me to use Irish moss in your boil to remove high Mw protein, then later add gelatine (a high Mw protein). Gelatine should complex with polyphenols to cause chill haze just like the original proteins would have. I started this thread (and my thinking about clarifiers) after getting lots of funky precipitate in bottles of a batch that used both IM and gelatine.
Clarifier pairs that make chemical sense to me:
irish moss/polyclar (remove proteins and polyphenols to REALLY kill chill haze)
polyclar/gelatine (remove polyphenols for chill haze, and drop excess yeast)
Jeff Jones
dwhi...@rohmhaas.com (Dave Whitman) wrote:
> Clarifier pairs that make chemical sense to me:
> irish moss/polyclar (remove proteins and polyphenols to REALLY kill chill
> haze)
This is what I do and it _really_ makes the beer clear.
Jim
(ok most of it) until the brew settles down. It usually takes a good
month.
--
Jim sends, www.ionet.net/~gator/index.shtml
Quote: I didn't have time..Translated..I didn't know what I was doing.
TF
Dave Foulser
or polyclar) in my secondary and getting very clear beer. The real
benefit is that the beer tastes much better, which I assume has to do
with reduced amounts of dead yeast.
Dave
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