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Access to Hydrogen Sulfide?
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Sara Ann Wylie  
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 More options May 2 2012, 5:59 pm
From: Sara Ann Wylie <sawy...@MIT.EDU>
Date: Wed, 02 May 2012 17:59:43 -0400
Local: Wed, May 2 2012 5:59 pm
Subject: Access to Hydrogen Sulfide?
Hi all,

We are getting ready to begin lab testing to calibrate our photographic paper
strips. For research notes on this see below. Unfortunately tanks of Hydrogen
Sulfide are quite costly. Does anyone have access to Hydrogen Sulfide? Or a
good protocol for making it in known quantities?

Cheers

Sara

Links to work on this project:

Description of what we have for the experimental set up:
http://publiclaboratory.org/notes/sara/4-2-2012/planning-public-lab-h...

Description of prior lab research on this tool:
http://publiclaboratory.org/notes/sara/3-30-2012/description-horwell-...

Draft Experimental Design:
http://publiclaboratory.org/notes/sara/4-2-2012/h2s-experimental-set-...


 
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Jeffrey Warren  
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 More options May 2 2012, 6:05 pm
From: Jeffrey Warren <j...@publiclaboratory.org>
Date: Wed, 2 May 2012 18:05:36 -0400
Local: Wed, May 2 2012 6:05 pm
Subject: Re: [PLOTS] Access to Hydrogen Sulfide?

A quick googling shows:

* http://en.wikipedia.org/wiki/Hydrogen_sulfide#Production
* http://forums.homesciencelab.com/viewtopic.php?f=7&t=72 (DIY)
*
http://www.sustainablesupply.com/MSA-711062-Calibration-Gas-40-Ppm-Hy...
for
$157

On Wed, May 2, 2012 at 5:59 PM, Sara Ann Wylie <sawy...@mit.edu> wrote:


 
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dick.spra...@comcast.net  
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 More options May 3 2012, 12:12 pm
From: dick.spra...@comcast.net
Date: Thu, 3 May 2012 16:12:02 +0000 (UTC)
Local: Thurs, May 3 2012 12:12 pm
Subject: Re: [PLOTS] Access to Hydrogen Sulfide?

Let's be careful, folks. Hydrogen sulfide is extremely dangerous (as one of the links in the email chain below indicates, it is similar to hydrogen cyanide {the execution gas} in toxicity). It should be generated with extreme care, only by a professional chemist, and only in a laminar flow hood to channel the hydrogen sulfide away from the person generating it. As another of the links in the email chain cites, it is also very difficult to generate a controlled flow of a constant concentration of H2S gas (both requirements for a standard gas solution). Generating hydrogen sulfide gas using a cookbook procedure and without proper protection is following a recipe for a potentially tragic death.

Hydrogen sulfide detectors are available for rental through various sources, and cost approx $25 per day. These detectors should come pre-calibrated and ready to use; if rented for multiple days, they should come with a calibration kit, including directions. See http://www.idealcalibrations.com/gas-detector-rental/ for one example. Rental agencies exist in almost every major city, so shipping costs should not apply.

These detectors are also available for sale, but then you would need to have the standard gas, and this would essentially double the first cost price to around $400 for just the H2S monitoring capability.

Is the public laboratory a 501(c)(3) organization? Could it qualify as a professional or educational organization, even if loosely affiliated? If yes, you might find vendors or other parties that are willing and able to donate this equipment, sell it at a discount, make a donation toward purchase, etc. in exchange for a tax write-off. I am currently a member of two 501(c)(3) organizations (ASTM.org and SWANA.org) which accept sponsorships from various vendors in exchange for access to members at defined times and places. I would be willing to help register the public laboratory as a 501(c)(3) organization if this seems worthwhile to accomplishing your goals.

Dick Sprague


 
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Shannon Dosemagen  
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 More options May 3 2012, 12:15 pm
From: Shannon Dosemagen <shan...@publiclaboratory.org>
Date: Thu, 3 May 2012 11:15:36 -0500
Local: Thurs, May 3 2012 12:15 pm
Subject: Re: [PLOTS] Access to Hydrogen Sulfide?

Thanks for your thoughts Dick! In regards to 501(c)(3) status, we have
filed the 1023 papers with the IRS and are waiting for a decision from
them. Best, Shannon

--
Shannon Dosemagen
Public Laboratory for Open Technology and Science
504.239.4642
publiclaboratory.org

 
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