NUS setup
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partha
Aug 23, 2011, 1:43:16 PM8/23/11
to mddnmr
Dear All,
I'm trying to setup NUS acquisition method for the solids MAS NMR
experiment in Bruker Avance 400MHz spectrometer with Topspin 3.0.
The experiment I'm trying to setup is 13C/13C 2D fp-RFDR experiment
which works well with the traditional data collection method.
I know I have to change the pulse program using the mc-syntax, not
quite sure how it works. Is it just sufficient to modify F1PH in the
pulse program to F1PH(calph,caldel). Any kind of help or suggestions
appreciated.
Thankyou
Sudhakar Parthasarathy
Graduate Student
Department of Chemistry
University of Illinois at Chicago
Chicago, IL
USA
I'm trying to setup NUS acquisition method for the solids MAS NMR
experiment in Bruker Avance 400MHz spectrometer with Topspin 3.0.
The experiment I'm trying to setup is 13C/13C 2D fp-RFDR experiment
which works well with the traditional data collection method.
I know I have to change the pulse program using the mc-syntax, not
quite sure how it works. Is it just sufficient to modify F1PH in the
pulse program to F1PH(calph,caldel). Any kind of help or suggestions
appreciated.
Thankyou
Sudhakar Parthasarathy
Graduate Student
Department of Chemistry
University of Illinois at Chicago
Chicago, IL
USA
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